[1]昝立峰,葛水莲,李丹花,等.大孔吸附树脂分离纯化紫甘薯色素的研究[J].黑龙江农业科学,2015,(12):116-119.[doi:10.11942/j.issn1002-2767.2015.12.0116]
ZAN Li-feng,GE Shui-lian,LI Dan-hua,et al.Preliminary Separation and Purification of Pigments from?Ipomoea batatas??(L.) Lam by Macroporous Resins[J].HEILONGJIANG AGRICULTURAL SCIENCES,2015,(12):116-119.[doi:10.11942/j.issn1002-2767.2015.12.0116]
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ZAN Li-feng,GE Shui-lian,LI Dan-hua,et al.Preliminary Separation and Purification of Pigments from?Ipomoea batatas??(L.) Lam by Macroporous Resins[J].HEILONGJIANG AGRICULTURAL SCIENCES,2015,(12):116-119.[doi:10.11942/j.issn1002-2767.2015.12.0116]
大孔吸附树脂分离纯化紫甘薯色素的研究
《黑龙江农业科学》[ISSN:1002-2767/CN:23-1204/S]
卷:
期数:
2015年12
页码:
116-119
栏目:
出版日期:
2015-12-10
- Title:
- Preliminary Separation and Purification of Pigments from?Ipomoea batatas??(L.) Lam by Macroporous Resins
- 文章编号:
- 1002-2767（2015）12-0116-04
- 分类号:
- TS202.3
- 文献标志码:
- A
- 摘要:
- 为了筛选出一种高吸附、高解吸性能大孔吸附树脂，比较了14种大孔吸附树脂对紫甘薯色素的静态吸附和解吸性能。在此基础上研究了吸附液pH、解吸流速、洗脱液浓度及pH对色素纯化的影响。结果表明：DM21树脂为分离纯化紫甘薯色素的最佳树脂，其最佳纯化条件是吸附液和解吸液pH2.0～4.0，解吸液乙醇浓度为70%，解吸液解析流速为3 Bv?h-1时，对紫甘薯色素的纯化效果以及效率最好，色价达到54.26±0.87。
- Abstract:
- The performances of pigments from Ipomoea batatas?(L.) Lam extracts on fourteen macroporous resins were investigated in order to optimize the separation process,different pH values of sample solution,different desorption velocities,different concentrations and pH values of ethanol solution also had been investigated.The results of static tests indicated that DM21 resin was the most appropriate,and the best conditions were adsorption velocity of 3 Bv,pH2.0~4.0,desorption solvent of 70% ethanol.The pigments content of purple potato extract purificated by DM21 resin were more than 54.26±0.87,in line with market requirements.
参考文献/References:
[1]杨朝霞,王亦军,高磊.紫甘薯花色苷色素研究进展[J].青岛大学学报,2004,19(2): 32-36.[2]Corrales M,Toepfl S,Butz P,et al.Extraction of anthocyanins from grape by products assisted by ultrasonicshigh hydrostatic pressure or pulsed electric fields:Acomparison[J].Innov Food Sci Emerg Technol,2008,9: 85-91.[3]刘学峰,石雷,郑文秀.紫番薯色素提取精制工艺的研究[J].中国食品添加剂,2009（6）:121-125.[4]翟彦青,李翠清,李建刚,等.紫甘薯色素提取工艺研究[J].北京石油化工学院学报,2012,20(3): 1-4.[5]陈勇,张晴.AB-8大孔吸附树脂吸附和分离紫甘薯色素的研究[J].中国食品添加剂， 2001（1）：6-9.
备注/Memo
收稿日期：2015-08-04基金项目：邯郸学院校内资助项目（14101）; 河北省高校冀南太行山区资源植物应用研发中心资助项目; 河北省科技计划资助项目（13222907）第一作者简介：昝立峰（1980-），男，内蒙古自治区乌兰察布市人，博士，讲师，从事天然产物研究。E-mail: tengfei007zlf@126.com。
更新日期/Last Update:
2016-12-08