[1]田梦飞,肖雨昕,刘庆龙,等.MOFs对毛蕊花糖苷的吸附解吸性能研究[J].黑龙江农业科学,2022,(05):74-79.[doi:10.11942/j.issn1002-2767.2022.05.0074]
　TIAN Meng-fei,XIAO Yu-xin,LIU Qing-long,et al.Exploration of the Adsorption and Desorption Performance of Acteoside on MOFs[J].HEILONGJIANG AGRICULTURAL SCIENCES,2022,(05):74-79.[doi:10.11942/j.issn1002-2767.2022.05.0074]
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MOFs对毛蕊花糖苷的吸附解吸性能研究

《黑龙江农业科学》[ISSN:1002-2767/CN:23-1204/S] 卷: 期数: 2022年05 页码: 74-79 栏目: 出版日期: 2022-05-10
Title:
Exploration of the Adsorption and Desorption Performance of Acteoside on MOFs
作者:
田梦飞1; 2; 3; 肖雨昕1; 2; 刘庆龙1; 2; 邱乐群1; 3; 4; 王伟豪1; 2; 3; 李春英1; 3; 4; 赵春建1; 2; 3
1.东北林业大学 化学化工与资源利用学院，黑龙江 哈尔滨 150040；2.林业生物制剂教育部工程研究中心，黑龙江 哈尔滨 150040；3.黑龙江省林源活性物质生态利用重点实验室，黑龙江 哈尔滨 150040；4.森林植物生态学教育部重点实验室，黑龙江 哈尔滨 150040
Author(s):
TIAN Meng-fei1; 2; 3; XIAO Yu-xin1; 2; LIU Qing-long1; 2; QIU Le-qun1; 3; 4; WANG Wei-hao1; 2; 3; LI Chun-ying1; 3; 4; ZHAO Chun-jian1; 2; 3
1.College of Chemical,Chemical Engineering and Resource Utilization,Northeast Forestry University,Harbin 150040,China; 2.Engineering Research Center of Forestry Biologics,Ministry of Education,Harbin 150040,China; 3.Heilongjiang Provincial Key Laboratory of Ecological Utilization of Forestry-based Active Substances,Harbin 150040,China; 4.Key Laboratory of Forest Plant Ecology,Ministry of Education,Northeast Forestry University,Harbin 150040,China
关键词:
MOFs; 分散固相萃取; 地黄叶; 毛蕊花糖苷; 大孔树脂
Keywords:
MOFs; dispersive solid phase extraction; leaves of Rehmannia glutinosa Libosch.; acteoside; macroporous resin
DOI:
10.11942/j.issn1002-2767.2022.05.0074
文献标志码:
A
摘要:
为了探究MOFs材料对地黄叶提取物中毛蕊花糖苷的吸附解吸性能，首先制备MOFs材料，随后以吸附量、解吸量、解吸率为指标筛选最适宜分离毛蕊花糖苷的MOFs和大孔树脂，以单因素试验对ZIF-8吸附、解吸毛蕊花糖苷的能力进行优化，并在优化所得条件下比较ZIF-8和D-101对毛蕊花糖苷的吸附、解吸能力。结果表明：ZIF-8对毛蕊花糖苷的吸附量和解吸量分别为40.78和25.42 mg·g-1，其分别是D-101大孔树脂对毛蕊花糖苷吸附量和解吸量的1.85倍和1.83倍。因此，ZIF-8对毛蕊花糖苷的吸附、解吸性能优于D-101大孔树脂。
Abstract:
In order to explore the adsorption and desorption properties of MOFs on acteoside in Rehmannia glutinosa leaves extract,MOFs were first prepared by referring to the literature method.Then,the most suitable MOFs and macroporous resins for the separation of acteoside were screened according to the adsorption capacity,desorption capacity and desorption yield.The ability of ZIF-8 to adsorb and desorb acteoside was optimized by single factor experiments.The adsorption and desorption capacities of ZIF-8 and D-101 on acteoside were compared under the optimized conditions.The results showed that the adsorption and desorption of acteoside by ZIF-8 were 40.78 and 25.42 mg·g-1,respectively.Which were 1.85-fold and 1.83-fold that of those obtained by D-101,respectively.Therefore,the adsorption and desorption performance of ZIF-8 on acteoside was better than that of D-101 macroporous resin.

参考文献/References:

［1］ZONG W R,CHEONG K L,WU D T,et al.Preparation and purification of raffinose family oligosaccharides from Rehmannia glutinosa Libosch.by fast protein liquid chromatography coupled with refractive index detection[J].Separation and Purification Technology,2014,138:98-103.

［2］ZHOU F,XU T,ZHAO Y J,et al.Chitosan-coated liposomes as delivery systems for improving the stability and oral bioavailability of acteoside[J].Food Hydrocolloids,2017,83:17-24.

［3］郑帅,杨敏,白彝华,等.毛蕊花糖苷调控Snail1表达在糖尿病肾脏疾病中上皮细胞-间质转化中的作用[J].中国老年学杂志,2021,41(19):4320-4324.

［4］谢莹,林鑫,袁静,等.毛蕊花糖苷对糖尿病肾病小鼠肾组织中高迁移率族蛋白1及核因子KB表达的影响[J].中华肾脏病杂志,2021,37(10):817-823.

［5］孔德兴,徐永清,杨燕,等.向日葵列当毛蕊花糖苷的提取工艺优化及其抗氧化活性[J/OL].西北农林科技大学学报(自然科学版),2022,50(8):1-11[2022-01-10].https://kns.cnki.net/kcms/detail/detail.aspx?dbcode=CAPJ&dbname=CAPJLAST&filename=XBNY20220120003&uniplatform=NZKPT&v=U7efZxBmFVBEbOLFZ3IU7dCjqETC3ODTxq_M7uS0lX-ErW33rs2Pw1-dRVnvOzwh.DOI:10.13207/j.cnki.jnwafu.2022.08.012.

［6］王唯,王冬晶,孙亮,等.MOFs材料声催化活性在工业废水处理中的应用进展[J/OL].工业水处理,2022：1-8[2022-01-10].https://kns.cnki.net/kcms/detail/detail.aspx?dbcode=CAPJ&dbname=CAPJLAST&filename=GYSC20220217000&uniplatform=NZKPT&v=WAyoBR-pUseTirUhvyjIS0I_YngGubQXccVojp7SFMVSxoyZy6zxzlxMtpt-zjPN.DOI:10.19965/j.cnki.iwt.2021-1356.

［7］张秋云,杨先菊,吴亚萍,等.MOFs衍生TiO2负载硅钨酸的制备及催化合成生物柴油[J].粮食与油脂,2022,35(1):58-63.

［8］田娜,贾庆明,马艾华,等.金属-有机骨架材料的微波法制备及其应用[J].化工新型材料,2016,44(10):39-41.

［9］杨宇州,李政,黄艳凤,等.MOF基水凝胶材料的制备及其应用[J].化学进展,2021,33(5):726-739.

［10］MOHAMED Y,QUYNH N P L,NORAFIQAH I,et al.Effect of incorporating different ZIF-8 crystal sizes in the polymer of intrinsic microporosity,PIM-1,forCO2/CH4 separation[J].Microporous and Mesoporous Materials,2021,312:110761.

［11］封红瑞,李松涛,霍晓兵,等.ZIF-8材料的制备及应用进展[J].化学通报,2021,84(12):1314-1322.

［12］COMBARIEU G,MORCRETTOT M,MILLANGE F,et al.Influence of the benzoquinone sorption on the structure and electrochemical performance of the MIL-53(Fe) hybrid porous material in a lithium-lon battery[J].Chemistry of Materials,2009,21(8):1602-1611.

［13］生森森,刘佳祥,李卓.金属有机框架材料UiO-66-(COOH)2吸附去除染料废水中的亚甲基蓝和罗丹明B[J].西安交通大学学报,2020,54(9):180-188.

备注/Memo

收稿日期：2022-01-28

基金项目:大学生创新训练项目（202110225447）。

第一作者：田梦飞 （1993-），女，硕士研究生，从事植物活性成分分离与活性研究。E-mail:1255894206@nefu.edu.cn。

通信作者：李春英（1976-），女，博士，副教授，从事植物活性成分分离与活性研究。E-mail：lcy@nefu.edu.cn。

更新日期/Last Update: 2022-07-15