[1]蒋冰清,罗盛东.HPLC法测定滇桂艾纳香中原儿茶酸和原儿茶醛的含量[J].黑龙江农业科学,2015,(03):120-122.[doi:10.11942/j.issn1002-2767.2015.03.0120]
　JIANG Bing-qing,LUO Sheng-dong.Determination of Protocatechuic Acid and Protocatechuic Aldehyde in Blumeae ripariaeby HLPC[J].HEILONGJIANG AGRICULTURAL SCIENCES,2015,(03):120-122.[doi:10.11942/j.issn1002-2767.2015.03.0120]
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HPLC法测定滇桂艾纳香中原儿茶酸和原儿茶醛的含量

《黑龙江农业科学》[ISSN:1002-2767/CN:23-1204/S] 卷: 期数: 2015年03 页码: 120-122 栏目: 出版日期: 2015-03-10
Title:
Determination of Protocatechuic Acid and Protocatechuic Aldehyde in Blumeae ripariaeby HLPC
文章编号:
1002-2767（2015）03-0120-03
作者:
蒋冰清; 罗盛东
广西万寿堂药业有限公司，广西 南宁 530219
Author(s):
JIANG Bing-qing; LUO Sheng-dong
Guangxi Medic Top Pharmaceutical Company Limited ，Nanning，Guangxi 530219
关键词:
高效液相色谱; 滇桂艾纳香; 原儿茶酸; 原儿茶醛
Keywords:
HLPC;  Blumeae ripariae; protocatechuic acid; protocatechuic aldehyde
分类号:
R284.1
DOI:
10.11942/j.issn1002-2767.2015.03.0120
文献标志码:
A
摘要:
为了测定壮药材滇桂艾纳香中原儿茶酸和原儿茶醛的含量，利用高效液相色谱法测定6批壮药滇桂艾纳香药材原儿茶酸和原儿茶醛的含量。结果表明：原儿茶酸、原儿茶醛分别在5.008～25.040及5.344～26.720 μg?mL-1范围内呈现良好的线性关系；原儿茶酸和原儿茶醛平均回收率分别为98.61%和98.07%，RSD分别为1.44%和1.99%。
Abstract:
To develop an HPLC method for determination of protocatochuic acid and protocatechuic aldehyde in Diangui’ ainaxiang，protocatechuic acid and protocatechuic aldehyde of Blumeae ripariae from six origin were determined by HLPC.The results showed that protocatechuic acid had linear relationship in the range of 5.008～25.04 μg， protocatechuic aldehydethe had linear relationship in the range of 5.344～26.72 μg ，the recovery was 98.61% and 98.07% respectively，RSD was 1.44% and 1.99% respectively.

参考文献/References:

［1］王治平，杨珂，孟祥平，等.RPHPLC法测定滇桂艾纳香中原儿茶酸与原儿茶醛的含量[J].中药材，2005，15(5):393-394.
 [2]郑维兵.RPHPLC法测定急支糖浆中原儿茶酸和原儿茶醛的含量[J] .儿科药学杂质，2010,16(4):51-52.
 [3]邢俊波，王朝红.HPLC法测定肺炎平胶囊中原儿茶酸和原儿茶醛的含量[J] .中国实验方剂杂质，2008（3）：8-12.

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备注/Memo

第一作者简介：蒋冰清（1984-），女，广西壮族自治区兴安县人，助理工程师，从事中成药及中药材的有效成分提取及质量分析研究。E-mail：274494130@qq.com。

更新日期/Last Update: 2017-02-10