CAI Yu-hong,FAN Hui-mei,ZHANG Zhi-xin,et al.Evaluation of Uncertainty of Determination of Exchangeable Potassium in Soil by Flame Photometry[J].HEILONGJIANG AGRICULTURAL SCIENCES,2016,(10):43-45.[doi:10.11942/j.issn1002-2767.2016.10.0043]
火焰光度法测定土壤中速效性钾含量的不确定度评定
- Title:
- Evaluation of Uncertainty of Determination of Exchangeable Potassium in Soil by Flame Photometry
- 文章编号:
- 1002-2767(2016)10-0043-03
- Keywords:
- soil; exchangeable potassium; evaluation of uncertainty
- 分类号:
- S158.2
- 文献标志码:
- A
- 摘要:
- 依据NY/T 889-2004标准,以中性乙酸铵作为浸提剂,用火焰光度计测定了土壤中速效钾的含量,建立数学模型。结果表明:确定测量不确定度的因素,评估各个不确定度分量,给出了该方法的标准合成不确定度及扩展不确定度,如实反映了测量的置信度和准确度。当土壤中速效性钾含量为183.2 mg·kg-1时,置信概率p=0.95时,本方法的标准合成不确定度为4.21 mg·kg-1,扩展不确定度为8.42 mg·kg-1(k=2)。
- Abstract:
- According to NY/T 889-2004,taking neutral ammonium acetate as the extraction agent,the content of available potassium in the soil was determined by using flame photometer,mathematics model was builded,elements of measurement uncertainty was identified,components of each uncertainty were evaluated,standard compound uncertainty and extension uncertainty of this method were put forward.When exchangeable potassium content of soil was 1.832 mg·kg-1,confidence probability p=0.95,standard compound uncertainty was 4.21 mg·kg-1,the extension uncertainty was 8.42 mg·kg-1(k=2)of this method.
参考文献/References:
[1]
张成梯
.
测量不确定度评定中的若干问题
[J].
中国测试技术
,2007,33(5):24-28.
[2] 倪育刁.实用测量不确定度评定[M].2版.北京:中国计量出版社,2007. [3] 国家质量技术监督局.JJF 1059.1-2012测量不确定度评定与表表示[S]. [4] 中国合格评定国家认可委员会.化学分析中不确定度的评估指南[M].北京:中国合格评定国家认可委员会,2006. [5] 中国实验室国家认可委员会.ISO/IEC 17025:2005检测和校准实验室认可准则[S].中国实验室国家认可委员会,2005. [6] NY/T 889-2004土壤速效钾和缓效钾含量的测定[S]. [7] JJG 630-2007《火焰光度计》[S]. [8] 国家质量技术监督局.JJG 196-2006常用玻璃量器检定规程[S].
相似文献/References:
[1]杨卫斌,唐静.黑龙江八五四农场农田土壤养分变化状况分析[J].黑龙江农业科学,2013,(02):48.
YANG Wei-bin,TANG Jing.Analysis on Farmland Soil Nutrient Status in 854 Farm of Heilongjiang Province[J].HEILONGJIANG AGRICULTURAL SCIENCES,2013,(10):48.
[2]马星竹.长期试验土壤理化性质和微生物量的研究进展[J].黑龙江农业科学,2013,(03):147.
MA Xing-zhu.Research Progress on Soil Physical and Chemical Property and Microbial Biomass of Long-term Experiment[J].HEILONGJIANG AGRICULTURAL SCIENCES,2013,(10):147.
[3]潘多锋,申忠宝,王建丽,等.紫花苜蓿与无芒雀麦混播对松嫩平原盐碱化草地土壤改良效果研究[J].黑龙江农业科学,2012,(10):127.
PAN Duo-feng,SHEN Zhong-bao,WANG Jian-li,et al.Study on Soil Improvement Effect of AlfalfaMixed with Smooth Brome Grass onSaline-Alkaline Grassland in Songnen Plain[J].HEILONGJIANG AGRICULTURAL SCIENCES,2012,(10):127.
[4]张爽,潘伟,王海峰,等.苹果梨园土壤养分状况调查与研究[J].黑龙江农业科学,2013,(04):31.
ZHANG Shuang,PAN Wei,WANG Hai-feng,et al.Investigation and Research on the Soil Nutrient in the Apple-pear Orchard[J].HEILONGJIANG AGRICULTURAL SCIENCES,2013,(10):31.
[5]王 麒.不同玉米栽培模式对土壤物理性状及产量影响的研究[J].黑龙江农业科学,2012,(08):25.
WANG Qi.Effect of Different Cultivation Models on Soil PhysicalProperties and Yield of Maize[J].HEILONGJIANG AGRICULTURAL SCIENCES,2012,(10):25.
[6]迟莉.黄绿木霉菌及其混剂对辣椒植株及土壤的影响[J].黑龙江农业科学,2013,(07):42.
CHI Li.Effects of Trichoderma aureoviride and its Agents on Hot Pepper Plants and Soil[J].HEILONGJIANG AGRICULTURAL SCIENCES,2013,(10):42.
[7]邹东月.黑龙江省农业科学院克山分院试验地土壤有效铜含量分析[J].黑龙江农业科学,2011,(02):37.
ZOU Dong-yue.Analysis of Available Cu Content in Soil of Keshan Branch ofHeilongjiang Academy of Agricultural Sciences[J].HEILONGJIANG AGRICULTURAL SCIENCES,2011,(10):37.
[8]黄 静,吴祥云,闫 晗.彰武县境内柳河所辖小流域土壤风蚀时空动态变化特征[J].黑龙江农业科学,2011,(02):45.
HUANG Jing,WU Xiang-yun,YAN Han.Spatial-temporal Dynamic Change Feature of Soil Wind Erosion inSmall Watersheds of the Liu River in Zhangwu County[J].HEILONGJIANG AGRICULTURAL SCIENCES,2011,(10):45.
[9]宋庆英,蔡 森,林 影.加强耕地质量建设 实现粮食稳产增产[J].黑龙江农业科学,2011,(04):120.
SONG Qing-ying,CAI Sen,LIN Ying.Enhancing the Quality Construction of Cultivated Land andMaking theProduction of Crop Increasing and Stable[J].HEILONGJIANG AGRICULTURAL SCIENCES,2011,(10):120.
[10]元 野,王光华,赵光伟,等.不同种植制度下烤烟根际土壤微生物群落结构的变化[J].黑龙江农业科学,2011,(11):26.
YUAN Ye,WANG Guang-hua,ZHAO Guang-wei,et al.Changes of Microbial Community Structure on Flue-cured Tobacco Soil Rhizosphere in Different Cropping Systems[J].HEILONGJIANG AGRICULTURAL SCIENCES,2011,(10):26.
备注/Memo
收稿日期:2016-09-17