JI Hui-jie,YANG Yan-jun,XUE Jun-li,et al.Study on Extraction Technology of Alion from Aloe by Ultrasonic[J].HEILONGJIANG AGRICULTURAL SCIENCES,2015,(02):94-97.[doi:10.11942/j.issn1002-2767.2015.02.0094]
超声波提取芦荟中芦荟苷的工艺研究
- Title:
- Study on Extraction Technology of Alion from Aloe by Ultrasonic
- 文章编号:
- 1002-2767(2015)02-0094-04
- Keywords:
- Aloe; aloin; ultrasonic-assisted extraction; orthogonal
- 分类号:
- TQ464.3
- 文献标志码:
- A
- 摘要:
- 为探讨提取芦荟中芦荟苷的最佳工艺条件,以芦荟苷含量为指标,超声波辅助法进行正交试验,确定芦荟苷提取工艺。结果表明:超声波提取的最佳工艺条件为:乙醇浓度80%,料液比1:55,超声温度35℃,超声时间40 min。在此条件下,用紫外分光光度法测定所提取芦荟苷的含量为8.520 mg?g-1。芦荟苷正交提取工艺的研究结果可靠。
- Abstract:
- In order to investigate the optimum conditions to extract aloin from Aloe,taking aloin content as an indicator,the effect of ultrasonic-assisted extraction on aloin in Aloe were studied,and the optimal extraction conditions was determined.The results showed that the optimum conditions for ultrasonic extraction: ethanol concentration was 80%,solid-liquid ratio was 1:55,uhrasonic temperature was 35℃ and uhrasonic time was 40 min.Determination of aloin by UV spectrophotometry,the extraction rate could reach 8.520 mg?g-1 under these conditions.The results of orthogonal extraction process of aloin were reliable.
参考文献/References:
[1]Dagne E,Bisrat D,Viljoen A,et al.Chemistry of Aloe species.current organic chemistry[J].2000,4(10):1055.
[2]岳银屏,吴强,邢旭.芦荟的稳定性研究[J].食品工业科技,2006,27(10):85.
[3]刘玉魁,郭赢霞,赵作连,等.药用芦荟中芦荟苷的提取分离及含量测定[J].医学导报,2009,26(4):413-414.
[4]王莲,吕芳,张荣泉.植物芦荟的化学成分、药理作用及应用的研究进展[J].天津药学,2009,21(2):63-64. [5]陈国和,刘玉鑫,张新申,等.芦荟的化学成分及其分离和分析[J].化学研究与应用,2002,4(2):133-135.[6]孙海燕,王绿娅,吕树.芦荟的化学成分与应用概况[J].中国药物应用与监,2004(2):40-41.
[7]罗秉俊,杨芳芳.库拉索芦荟凝胶加工过程中芦荟苷的控制[J].中国农村科技,2009(3):78-79.
[8]马稳,宋力.超声提取芦荟中芦荟苷的工艺研究[J].食品工艺科技杂志,2008(9):191-194.
[9]李培,陈少明.超声波辅助萃取芦荟中蒽醌类化合物工艺研究[J].安徽农业科学,2010,38(11):5867.[10]裴正玲,孙婷婷.黄锁义超声波提取芦荟总黄酮及其鉴别[J].微量元素与健康研究,2007,24(1):26-27. [11]曾云瑾.芦荟甙含量测定方法概况[J].蛇志,2006,18(3):210-212.
[12]刘玉魁,郭迎霞,赵作连,等.药用芦荟中芦荟苷的提取分离及含量测定[J].医药导报,2007,26(4):413-414.
备注/Memo
收稿日期:2014-06-23
第一作者简介:吉惠杰(1973-),女,吉林省吉林市人,学士,实验师,从事精细有机合成与应用方面的研究。E-mail:jihuijie70@126.com。