[1]马　利,孙长华,李春娟.反相高效液相色谱法测定土壤中甲黄隆残留[J].黑龙江农业科学,2009,(05):65-66.[doi:10.11942/j.isn1002-2767.2009.05.0065]
　MA Li,SUN Chang-hua,LI Chun-juan.Determination for Metsulfuron Residue in Soil by High PerformanceLiquid Chromatography[J].HEILONGJIANG AGRICULTURAL SCIENCES,2009,(05):65-66.[doi:10.11942/j.isn1002-2767.2009.05.0065]
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反相高效液相色谱法测定土壤中甲黄隆残留

《黑龙江农业科学》[ISSN:1002-2767/CN:23-1204/S] 卷: 期数: 2009年05 页码: 65-66 栏目: 出版日期: 2009-09-10
Title:
Determination for Metsulfuron Residue in Soil by High PerformanceLiquid Chromatography
文章编号:
1002-2767(2009)05-0065-02
作者:
马　利; 孙长华; 李春娟
(黑龙江省质量监督检测研究院,黑龙江哈尔滨 150050)
Author(s):
MA Li; SUN Chang-hua; LI Chun-juan
(Heilongjiang Provincial Quality Supervision and Test Institute,Harbin,Heilongjiang 150050)
关键词:
高效液相色谱法; 土壤; 残留; 甲黄隆
Keywords:
HPLC; soil; residue; metsulfuron
分类号:
O658
DOI:
10.11942/j.isn1002-2767.2009.05.0065
文献标志码:
A
摘要:
建立了反相高效液相色谱测定土壤中甲黄隆残留量的方法。 试验以甲醇∶水∶冰乙酸(60∶40∶1, 体积比)为流动相进行洗脱, 采用 C 18 柱分离,利用紫外检测器在 227nm 波长下检测。该方法在0.50～ 10.0mg·L -1 范围内呈良好线性, 相关系数为 0.9997, 检测限为0.005 mg·kg -1 , 方法的回收率为 86%～ 98%, 精密度为2.32%～ 4.04%, 用于土壤中甲黄隆残留检测效果良好
Abstract:
The high performance liquid chromatography method was developed for the determination of metsulfuron in soil.The chromatographic analysis was carriedout using the mobile phase consistedof methanol, water and acetic acid(60∶40∶1, v/ v), and the detection at 227 nm.The linear range was 0.50～ 10.0 mg·L -1 , and the detection limit was 0.005 mg·kg -1 ,spiked recoveries rate was 86%～ 98%, and the RSDs was 2.32%～ 4.04%.This method operated simple and detectioneffect of metsulfuron in soil was good.

参考文献/References:

[ 1] 　邓金保.黄酰脲类除草剂综述[ J] .世界农药,2003,25(3):224-229.

[ 2] 　郎印海, 蒋新,赵其国, 等.黄酰脲除草剂在土壤中的环境行为研究进展[ J] .应用生态学报, 2002, 13(9):1187-1190.
[ 3] 　刘志坚,陈道文, 蒋木庚, 等.甲黄隆在麦田的残留动态研究[ J] .南京农业大学学报, 1993, 16(2):96-99.

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备注/Memo

第一作者简介:马利(1953-),女,辽宁省辽阳市人, 高级实验师, 主要从事质量管理工作。E-mail:lidg86@yahoo.com.cn。

更新日期/Last Update: 2016-11-27