[1]姜少娟,王胜男,刘晓莉.响应面法优化香樟叶总黄酮的超声提取工艺[J].黑龙江农业科学,2018,(06):90-97.[doi:10.11942/j.issn1002-2767.2018.06.0090]
　JIANG Shao-juan,WANG Sheng-nan,LIU Xiao-li.Optimization of Ultrasound-assisted Extraction of Flavonoids from Cinnamomum camphora Leaves Using Response Surface Methodology[J].HEILONGJIANG AGRICULTURAL SCIENCES,2018,(06):90-97.[doi:10.11942/j.issn1002-2767.2018.06.0090]
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响应面法优化香樟叶总黄酮的超声提取工艺

《黑龙江农业科学》[ISSN:1002-2767/CN:23-1204/S] 卷: 期数: 2018年06期 页码: 90-97 栏目: 出版日期: 2018-06-10
Title:
Optimization of Ultrasound-assisted Extraction of Flavonoids from
Cinnamomum camphora Leaves Using Response Surface Methodology
作者:
姜少娟1; 2; 王胜男1; 2; 刘晓莉1; 2
1.攀枝花学院 生物与化学工程学院， 四川 攀枝花 617000；2.攀枝花市干热河谷特色生物资源工程技术中心， 四川 攀枝花617000
Author(s):
JIANG Shao-juan1; 2; WANG Sheng-nan1; 2; LIU Xiao-li1; 2
1.Department of Biology and Chemistry Engineering, Panzhihua University, Panzhihua 617000,China；2.The Engineering Center of Characteristic Biological Resources of Panzhihua Dry-hot Valley, Panzhihua 617000,China
关键词:
香樟叶; 总黄酮; 超声提取; 响应面法
Keywords:
Cinnamomum camphora leaves;  total flavonoids;  ultrasonic extraction;  response surface methodology
DOI:
10.11942/j.issn1002-2767.2018.06.0090
文献标志码:
A
摘要:
为了优化香樟叶中黄酮类化合物的提取工艺，以香樟叶为原料进行超声波辅助提取，以单因素试验的结果为依据，通过响应面分析法以乙醇浓度、料液比、超声提取时间以及提取温度等4个因素及其交互作用对香樟叶总黄酮提取效果的影响进行优化。结果表明：香樟叶中总黄酮的最佳提取工艺是乙醇浓度62%、料液比为1:10、在57 ℃ 条件下超声提取10 min。黄酮的提取率为42.35%。
Abstract:
In order to optimize flavonoids extraction process from Cinnamomum camphora leaves, we took Cinnamomum camphora leaves as raw material, using ultrasonic-assistant extraction, adopted single factor test and the response surface methodology(RSM)to optimize the effect of the solvent concentration, ratio of liquid to material, ultrasound time,ultrasound temperature on the extraction efficiency of total flavonoids. The results showed that the ethanol concentration was 62%, the ratio of feed liquid was 1∶10 and extraction temperature was 57 ℃, the extracting time was 10 min, under this condition, and the amount of extracted flavonoids was 42.35%.

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备注/Memo

收稿日期：2018-02-08基金项目：四川省教育厅一般资助项目（16ZB0471）。第一作者简介：姜少娟（1979-），女，硕士，副教授，从事天然产物化学方面的研究。E-mail:remonica@163.com。

更新日期/Last Update: 2018-09-12